SurfacePreparationforStrainGageBonding
Document No.:11129 1 of 7 Revision 19-Dec-11
Micro-Measurements [email protected] www.micro-measurements.com
Instruction Bulletin B-129-8
Micro-Measurements
SurfacePreparationforStrainGageBonding
1.0 Introduction
Straingagescanbesatisfactorilybondedtoalmostany
solidmaterialifthematerialsurfaceisproperlyprepared.
Whileaproperlypreparedsurfacecanbeachievedinmore
thanoneway,thespecificproceduresandtechniques
describedhereofferanumberofadvantages.Tobeginwith,
theyconstituteacarefullydeveloped
andthoroughlyproven
system;and,whentheinstructionsarefollowedprecisely
(alongwiththoseforgageandadhesivehandling),the
consistentresultwillbestrongstablebonds.Theprocedures
aresimpletolearn,easytoperform,andreadilyreproducible.
Furthermore,thesurfacepreparationmaterialsusedinthese
proceduresare,unlessotherwisenoted,generallylowin
toxicity,anddonotrequirespecialventilationsystemsor
otherstringentsafetymeasures.Ofcourse,aswithany
materialscontainingsolventsorproducingvapors,adequate
ventilationisnecessary.
Theimportanceofattentiontodetail,andpreciseadherence
toinstructions,cannotbeoverstressedinsurfacepreparation
for
straingagebonding.Lessthorough,orevencasual,
approachestosurfacepreparationmaysometimesyield
satisfactorygageinstallations;butforconsistentsuccessin
achievinghighqualitybonds,themethodsgivenherecan
berecommendedwithoutqualification.Fundamentaltothe
MicroMeasurementssystemofsurfacepreparation
isanunderstandingofcleanliness
andcontamination.All
opensurfacesnotthoroughlyandfreshlycleanedmustbe
consideredcontaminated,andrequirecleaningimmediately
priortogagebonding.Similarly,itisimperativethatthe
materialsusedinthesurfacepreparationbefresh,clean,
anduncontaminated.Itisworthnotingthatstraingagesas
receivedfromMicroMeasurementsarechemically
clean,andspeciallytreatedontheundersidetopromote
adhesion.Simplytouchingthegageswiththefingers
(whicharealwayscontaminated)canbedetrimentalto
bondquality.
TheMicroMeasurementssystemofsurfacepreparation
includesfivebasicoperations.Theseare,intheusual
orderofexecution:
1.Solvent
degreasing
2.Abrading(dryandwet)
3.Applicationofgagelayoutlines
4.Conditioning
5.Neutralizing
Thesefiveoperationsarevariedandmodifiedforcompatibility
withdifferenttestmaterialproperties,andexceptions
areintroducedasappropriateforcertainspecialmaterials
andsituations.
Thesurfacepreparationoperationsaredescribedindividually
in
Section2.0,followingasummaryofthegeneral
principlesapplicabletotheentireprocess.Section3.0
discussesspecialprecautionsandconsiderationswhichshould
beborneinmindwhenworkingwithunusualmaterials
and/orsurfaceconditions.
Thevarioussurfacepreparationandinstallationaccessories
referredtothroughoutthisApplicationNoteare
Micro
MeasurementsAccessories,listedinStrainGage
AccessoriesDataBookandavailabledirectlyfromMicro
Measurements.
Asaconveniencetothegageinstallerinquicklydetermining
thespecificsurfacepreparationstepsapplicabletoany
particulartestmaterial,Section4.0includesachartlisting
approximately75common(anduncommon)materialsand
thecorresponding
surfacepreparationtreatments.
2.0BasicSurfacePreparation
OperationsandTechniques
2.1GeneralPrinciplesofSurface
PreparationforStrainGageBonding
Thepurposeofsurfacepreparationistodevelopachemically
cleansurfacehavingaroughnessappropriatetothe
gageinstallationrequirements,asurfacealkalinity
correspondingtoapHof
7orso,andvisiblegagelayoutlines
forlocatingandorientingthestraingage.Itistowardthis
purposethattheoperationsdescribedherearedirected.
Asnotedearlier,cleanlinessisvitalthroughoutthesurface
preparationprocess.Itisalsoimportanttoguardagainst
recontaminationofaoncecleanedsurface.
Followingare
severalexamplesofsurfacerecontaminationtobeavoided:
a.Touchingthecleanedsurfacewiththefingers.
b.Wipingbackandforthwithagauzesponge,orreusinga
onceusedsurfaceofthesponge(orofacottonswab).
c.Draggingcontaminantsintothecleanedareafromthe
uncleanedboundaryofthatarea.
d.Allowingacleaningsolutiontoevaporateonthesurface.
e.Allowingacleanedsurfacetositformorethanafew
minutesbeforegageinstallation,orallowingapartially
preparedsurfacetositbetweenstepsinthecleaning
procedure.
Beyondtheabove,itis
goodpracticetoapproachthesurface
preparationtaskwithfreshlywashedhands,andtowash
handsasneededduringtheprocedure.
2.2SolventDegreasing
Degreasingisperformedtoremoveoils,greases,organic
contaminants,andsoluablechemicalresidues.Degreasing
shouldalwaysbethefirstoperation.Thisistoavoidhaving
subsequent
abradingoperationsdrivesurfacecontaminants
intothesurfacematerial.Porousmaterialssuchastitanium,
SurfacePreparationforStrainGageBonding
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Instruction Bulletin B-129-8
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castiron,andcastaluminummayrequireheatingtodrive off
absorbedhydrocarbonsorotherliquids.
Degreasingcanbeaccomplishedusingahotvapordegreaser,
anultrasonicallyagitatedliquidbath,aerosoltypespraycans
ofCSM2Degreaser,orwipingwithGC6IsopropylAlcohol.
Onewayapplicators,suchasthe
aerosoltype,ofcleaning
solventsarealwayspreferablebecausedissolvedcontaminants
cannotbecarriedbackintotheparentsolvent.Whenever
possible,theentiretestpieceshouldbedegreased.Inthecase
oflargebulkyobjectswhichcannotbecompletelydegreased,
anareacovering4to6in[100to150mm]onallsidesofthe
gageareashouldbecleaned.Thiswillminimizethechanceof
contaminationinsubsequentoperations,andwillprovidean
areaadequatelylargeforapplyingprotectivecoatingsinthe
finalstageofgageinstallation.
2.3SurfaceAbrading
GeneralInpreparationforgageinstallation,thesurface
is
abradedtoremoveanylooselybondedadherents(scale,rust,
paint,galvanizedcoatings,oxides,etc.),andtodevelopa
surfacetexturesuitableforbonding.Theabradingoperation
canbeperformedinavarietyofways,dependinguponthe
initialconditionofthesurfaceandthedesiredfinishforgage
installation.For
roughorcoarsesurfaces,itmaybenecessary
tostartwithagrinder,discsander,orfile.(Note:Before
performinganyabradingoperations,seeSection3.1forsafety
precautions.)Finishabradingisdonewithsiliconcarbidepaper
oftheappropriategrit,andrecommendedgritsizesforspecific
materialsaregiveninSection4.0.
Ifgritblastingisusedinsteadofabrading,eithercleanalumina
orsilica(100to400grit)issatisf actory.Inanycase,theair
supplyshouldbewellfilteredtoremoveoilandother
contaminantvaporscomingfromtheaircompressor.
Thegritusedinblasting
shouldnotberecycledorused
againinsurfacepreparationforbondingstraingages.
Theoptimumsurfacefinishforgagebondingdepends
somewhatuponthenatureandpurposeoftheinstallation.
Forgeneralstressanalysisapplications,arelativelysmooth
surface(intheorderof100μin[2.5μm]rms)issuitable,
andhastheadvantageoverroughersurfacesthatitcanbe
cleanedmoreeasilyandthoroughly.Smoothersurfaces,
compatiblewiththethin"gluelines"requiredforminimum
creep,areusedfortransducerinstallations.Incontrast,
whenveryhighelongationsmustbemeasured,arougher
(andpreferablycrosshatched)surfaceshouldbe
prepared.
Therecommendedsurfacefinishesforseveralclassesof
gageinstallationsaresummarizedinTableI,below.
TABLEI
CLASSOF
INSTALLATION
SURFACEFINISH,rms
µin µm
Generalstressanalysis 63125 1.63.2
Highelongation
>250 >6.4
crosshatched
Transducers 1663 0.41.6
WetAbradingWheneverMPrepConditionerAis
compatiblewiththetestmaterial(seeSection4.0),the
abradingshouldbedonewhilekeepingthesurfacewetwith
thissolution,ifphysicallypracticable.ConditionerAisa
mildlyacidicsolutionwhichgenerallyacceleratesthecleaning
processand,onsomematerials,
actsasagentleetchant.Itis
notrecommendedforuseonmagnesium,syntheticrubber,or
wood.
2.4GageLocationLayoutLines
Thenormalmethodofaccuratelylocatingandorientinga
straingageonthetestsurfaceistofirstmarkthesurface
withapairofcrossedreferencelines
atthepointwherethe
strainmeasurementistobemade.Thelinesaremade
perpendiculartooneanother,withonelineorientedinthe
directionofstrainmeasurement.Thegageistheninstalled
sothatthetriangularindexmarksdefiningthelongitudinal
andtransverseaxesofthegridarealigned
withthereference
linesonthetestsurface.
Thereference,orlayout,linesshouldbemadewithatoolthat
burnishes,ratherthanscoresorscribes,thesurface.Ascribed
linemayraiseaburrorcreateastressconcentration.Ineither
case,suchalinecanbedetrimentaltostraingage
performanceandtothefatiguelifeofthetestpart.On
aluminumandmostothernonferrousalloys,a4Hdrafting
pencilisasatisfactoryandconvenientburnishingtool.
However,graphitepencilsshouldneverbeusedonhigh
temperaturealloys,wheretheoperatingtemperaturemight
causeacarbonembrittlement
problem.Ontheseandother
hardalloys,burnishedalignmentmarkscanbemadewitha
ballpointpenoraroundpointedbrassrod.Layoutlinesare
ordinarilyappliedfollowingtheabradingoperationandbefore
finalcleaning.Allresiduefromtheburnishingoperationshould
beremovedbyscrubbingwithConditionerAasdescribedin
thefollowingsection.
2.5SurfaceConditioning
Afterthelayoutlinesaremarked,ConditionerAshouldbe
appliedrepeatedly,andthesurfacescrubbedwithcotton
tippedapplicatorsuntilacleantipisnolongerdiscolored
bythescrubbing.Duringthisprocessthesurfaceshouldbe
keptconstantlywetwith
ConditionerAuntilthecleaningis
completed.Cleaningsolutionsshouldneverbeallowedto
dryonthesurface.Whenclean,thesurfaceshouldbedried
bywipingthroughthecleanedareawithasingleslow
strokeofagauzesponge.Thestrokeshouldbegininside
SurfacePreparationforStrainGageBonding
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thecleanedareatoavoiddraggingcontaminantsinfromthe
boundaryofthearea.Then,withafreshsponge,asingle
slowstrokeismadeintheoppositedirection.Thesponge
shouldneverbewipedbackandforth,sincethismayredeposit
thecontaminantsonthecleanedsurface.
2.6Neutralizing
Thefinalstepinsurfacepreparationistobringthesurface
conditionbacktoanoptimumalkalinityof7.0to7.5pH,
whichissuitableforallMicroMeasurementsstrain
gageadhesivesystems.Thisshouldbedonebyliberally
applyingMPrepNeutralizer5Atothecleanedsurface,and
scrubbingthesurface
withacleancottontippedapplicator.
Thecleanedsurfaceshouldbekeptcompletelywetwith
Neutralizer5Athroughoutthisoperation.Whenneutralized,
thesurfaceshouldbedriedbywipingthroughthecleaned
areawithasingleslowstrokeofacleangauzesponge.
Withafreshsponge,asinglestrokeshouldthenbemadein
theoppositedirection,beginningwiththecleanedareato
avoidrecontaminationfromtheuncleanedboundary.
Iftheforegoinginstructionsarefollowedprecisely,thesurface
isnowproperlypreparedforgagebonding,andthe
gageorgagesshouldbeinstalledassoonaspossible.
3.0Special
PrecautionsandConsiderations
3.1SafetyPrecautions
Asinanytechnicalactivity,safetyshouldalwaysbea
primeconsiderationinsurfacepreparationforstraingage
bonding.Forexample,whengrinding,discsanding,or
filing,theoperatorshouldwearsafetyglassesandtakesuch
othersafetyprecautionsasspecifiedbyhisorganization
or
bytheOccupationalSafetyandHealthAdministration
(OSHA).
Whendealingwithtoxicmaterialssuchasberyllium,lead,
uranium,plutonium,etc.,allproceduresandsafetymeasures
shouldbeapprovedbythesafetyofficeroftheestablishment
beforecommencingsurfacepreparation.
3.2SurfacesRequiringSpecialTreatment
ConcreteConcretesurfacesare
usuallyuneven,rough,
andporous.Inordertodevelopapropersubstrateforgage
bonding,itisnecessarytoapplyalevelingandsealingprecoat
ofepoxyadhesivetotheconcrete.Beforeapplyingthe
precoat,theconcretesurfacemustbepreparedbya
procedurewhichaccountsfortheporosityofthis
material.
Contaminationfromoils,greases,plantgrowth,andother
soilsshouldberemovedbyvigorousscrubbingwitha
stiffbristledbrushandamilddetergentsolution.Thesurface
isthenrinsedwithcleanwater.Surfaceirregularities
canberemovedbywirebrushing,discsanding,orgritblasting,
afterwhichallloosedustshouldbeblownorbrushed
fromthesurface.
ThenextstepistoapplyConditionerAgenerouslytothe
surfaceinandaroundthegagingarea,andscrubthearea
withastiffbristledbrush.ContaminatedConditionerA
shouldbeblottedwithgauzesponges,andthenthesurface
shouldberinsedthoroughlywithcleanwater.Following
thewaterrinse,thesurfaceaciditymustbereducedby
scrubbingwithNeutralizer5A,blottingwithga uzesponges,
andrinsingwithwater.Afinalthoroughrinsewith
distilledwaterisusefultoremovetheresidualtracesof
watersolublecleaningsolutions.Beforeprecoating,the
cleanedsurfacemustbethoroughlydried.Warmingthe
surfacegentlywithapropanetorchorelectricheatgunwill
hastenevaporation.
MicroMeasurementsMBondAE10roomtemperaturecuring
epoxyadhesiveisanidealmaterialforprecoatingthe
concrete.Forthosecasesinwhichthetesttemperaturemay
exceedthespecifiedmaximumoperatingtemperatureofAE
10(+200°F[+95°C]),itwillbenecessarytofillthesurfacewith
ahighertemperatureresinsystemsuchasMBondGA61.
Inapplyingthecoatingtotheporousmaterial,theadhesive
shouldbeworkedintoanyvoids,andleveledtoformasmooth
surface.Whentheadhesiveiscompletelycured,itshouldbe
abradeduntilthebasematerialbeginstobeexposedagain.
Followingthis,theepoxysurfaceiscleanedandprepared
conventionally,accordingtothe procedurespecifiedinSection
4.0forbondinggagestoepoxies.
PlatedSurfacesIngeneral,
platedsurfacesaredetrimental
tostraingagestability,anditispreferabletoremovethe
platingatthegagelocation,ifthisispermissible.Cadmium
andnickelplatingareparticularlysubjecttocreep,andeven
harderplatingsmaycreepbecauseoftheimperfectbond
betweentheplatingandthebasemetal.
Whenitisnot
permissibletoremovetheplating,thesurfaceshouldbe
preparedaccordingtotheproceduregiveninSection4.0
forthespecificplatinginvolved.Notethatitmaybenecessary
toadjusttestingprocedurestominimizetheeffectsof
creep.
UseofSolventsonPlasticsPlastics
varywidelyintheir
reactivitytosolventssuchasthoseemployedinthesurface
preparationproceduresdescribedhere.Beforeapplyinga
solventtoanyplastic,Section4.0,whichincludesmost
commonplastics,shouldbereferredtofortherecommended
compatiblesolvent.ForplasticsnotlistedinSection
4.0,themanufacturer
ofthematerialshouldbeconsulted,
ortestsshouldbeperformedtoverifynonreactivitybetween
thesolventandtheplastic.
DimensionalorMechanicalChangesDuetoSurface
PreparationFormostmaterials,strainmeasurementresults
areusuallynotsignificantlychan gedbythesurface
preparationproceduresdescribedinthisApplicationNote.
Even
withappreciablematerialremoval,effectsonthestatic
mechanicalpropertiesofthetestpartaregenerallynegligi‐
blecomparedtoothererrorsourcesintheexperiment.It
SurfacePreparationforStrainGageBonding
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shouldbeunderstood,however,thatremovalofaplatedor
hardenedsurfacelayer,orofasurfacelayerwithsignificant
residualstresses,maynoticeablyaffectthefatiguelifeor
thewearcharacteristicsofthepartwhenoperatedunder
dynamicserviceconditions.
SiliconeContamination—Thepropertiesofsilicones
whichmakethemexcellent
lubricantsandmoldrelease
agentsalsomakethemtheenemiesofadhesion,and
thereforepotentiallythemostseriousofcontaminantstobe
encounteredinthepracticeofbondingstraingages.The
problemiscompoundedbythehighnaturalaffinityof the
siliconesformostmaterials,andbytheirtendencyto
migrate.Furthermore,sincesiliconesarerelativelyinert
chemically,andunaffectedbymostsolvents,theyare
amongthemostdifficultsurfacecontaminantstoremove.
Thebestpracticeistokeepthegagebondingareafreeof
silicones.Thismaynotbeaseasyasitsounds,sincethe
widelyusedsiliconescanbeintroducedfromavarietyof
sources.Forinstance,manyhandcreamsandcosmetics
containsilicones,andtheseshouldnotbeusedbypersons
involvedingageinstallation.Someofthemachininglubricants
alsocontainsilicones,andsuchlubricantsshouldbe
avoidedwhenmachiningpartsthataretohavestrain
gages
installed.Similarly,siliconesaturatedcleaningtissuesfor
eyeglassesshouldnotbeusedinthegagebondingareaor
bygageinstallationpersonnel.
Regardlessofeffortstoavoidsilicones,contaminationmay
stilloccur.Lightcontaminationcansometimesberemoved
bycleaningwithConditionerA,preferablyheatedto
+200°F[+95°C].Moreseverecasesmayrequirespecial
cleaningsolutionsandprocedures,recommendationsfor
whichshouldbeobtainedfromthemanufacturerofthe
siliconecompoundinvolvedinthecontamination.
4.0IndexofTestMaterialsand
SurfacePreparationProcedures
Inthissection,thespecificstepbystepsurfacepreparation
proceduresaregivenforapproximately75
differentmaterials.
Forcompactness,andconvenient,quickaccesstothe
procedureforanyparticularmaterial,theinformationis
presentedinchartforminTableII.Thetestmaterialsare
listedalphabetically,fromABSPlasticstoZirconium;and
thecompleteprocedureforeachmaterialisdefinedbyone
ormoredigits
ineachoftheapplicableoperations columns
ofthetable.Eachdigitidentifiestherequiredoperationand
specifiesthestepnumberforthatoperationinthecomplete
procedure.
Forexample,assumethatthenecessityarisesforbonding
oneormorestraingagestoabrasstestspecimen.Reading
downtheSpecimen
MaterialcolumnofTableIItoBrass,
andfollowingthatrowacrossthetabletotheright,thefirst
stepinsurfacepreparationconsistsofdegreasingthe
specimenwithCSM2Degreaser.Thesymbol(1)inthe
IsopropylAlcoholcolumnindicatesthatthisisasuitable
substitutedegreasingoperation.Continuing
acrosstherow,
thesecondoperationcallsforabradingthespecimensurface
with320gritsiliconcarbidepaper.Inthethirdoperation
thespecimenisreabradedwith400gritsiliconcarbide
paper,wetlappingwithConditionerAiffeasible.The
fourthandfifthoperationsconsistofapplyinglayoutlines
forlocating
thegages,andscrubbingthesurfacecleanwith
ConditionerA.Cleaningwithisopropylalcoholisthefinal
operationintheprocedure.
IntheRemarkscolumn,itisrecommendedthatthegages
beinstalledwithin20minutesaftercompletingthesurface
preparation,becausethefreshlybaredbrasssurfacetendsto
oxidize
rapidly.Inaddition,intheGritBlastcolumn,the
gageinstallerisspecificallyadvisednottosubstitutegrit
blastingforothersurfaceabradingmethods,inorderto
avoidsignificantlyalteringthesurfaceconditionofthis
relativelysoftmaterial.Surfacepreparationproceduresfor
othermaterialsaredefinedsimilarlyinthetable,and,in
manycases,accompaniedbyspecialwarningsor
recommendationsintheRemarkscolumn.Whenanoperation
notincludedinthefirsttencolumnheadingsisrequired,itis
indexedintheOthercolumn,withanarrowpointingtothe
Remarkscolumnwheretheoperationisspecified.
AdditionalReferences
Foradditional
information,refertoInstructionBulletins
listedbelow:
B127,"StrainGageInstallationswithMBond200Adhesive".
B130,"StrainGageInstallationswithMBond43B,600,
and610Adhesives".
B137,"StrainGageApplicationswithMBondAE10,
AE15,andGA2AdhesiveSystems".
ImportantNotice
Theprocedures,operations,andchemicalagents
recommendedinthisApplicationNoteare,tothe
bestknowledgeofMicroMeasurements,
reliableandfitforthepurposesforwhichrecommended.
Thisinformationonsurfacepreparationforstraingage
bondingispresentedingoodfaithasanaidtothestrain
gageinstaller;butnowarranty,expressedorimplied,is
given,norshallMicroMeasurementsbeliableforany
injury,loss,ordamage,directorconsequential,connected
withtheuseoftheinformation.Beforeapplyingthe
procedurestoanymaterial,theuserisurgedtocarefully
reviewtheapplicationwithrespecttohuman
healthandsafety,andtoenvironmentalquality
SurfacePreparationforStrainGageBonding
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Micro-Measurements
TABLEII
IndexofTestMaterialsandSurfacePreparationProcedures(Sheet1of3)
SurfacePreparationforStrainGageBonding
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Instruction Bulletin B-129-8
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IndexofTestMaterialsandSurfacePreparationProcedures(Sheet2of3)
SurfacePreparationforStrainGageBonding
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Micro-Measurements
IndexofTestMaterialsandSurfacePreparationProcedures(Sheet3of3)